【国外标准】 Standard Guide for Development of Laser Diffraction Particle Size Analysis Methods for Powder Materials

5.1 The technique of laser diffraction for particle size distribution analysis is extensively used in industry and academia both for on-line control and laboratory needs. Guidance is obviously useful in this regard.5.2 This guide can be used to develop methods of particle size analysis where well-established analysis procedures do not already exist. See Guide B821 for similar guidance and useful procedures for wet dispersion of metal powders and related compounds.1.1 This guide sets out the general approach to the particle size distribution measurement of powders, suspensions, or slurries using an appropriate wet or dry methodology by the laser diffraction technique. It is recommended for use in measurements of broad particle size distributions.1.2 The guide provides guidelines to the parameters that should be specified and a generalized guideline to reasonable and acceptable tolerances for points in the volume-based distribution curve such as x10 (Dv10), x50 (Dv50), x90 (Dv90), and D[4, 3] (volume moment mean). It is noted that ISO prefers the term x for particle size as opposed to other usage of d or D (implying diameter).1.3 This guide provides guidance on the verification of instrument performance in conjunction with the internal quality control (QC) audit functions of the instrument owner. Results should be reported in the format indicated by Practice E1617 and ISO 13320.1.4 Units—The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.